Chemistry IA Exemplar: Dichloromethane Extraction Cycles and… | RevisionDojo
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IB Chemistry SL Internal Assessment Example
How does the number of dichloromethane extraction cycles (1, 2, 3, 4) with a fixed volume influence the total mass of caffeine extracted from coffee?SL
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5
Official IB Result
14/24
General feedback
14/24
0
12
24
No overall summary is available for this report.
5.1·Weakness
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The second figure’s caption repeats the same error. Ensure both structures reference a reliable chemical database, with correct spelling and source details.
5.2·Weakness
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Caption cites ‘Wikepedia.com’ with spelling errors and lacks a DOI or author. Replace with a peer‐reviewed source and correct citation format.
5.3·Weakness
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Hypothesis is plausible but could be sharpened. Clarify why the concentration gradient hypothesis predicts a logarithmic rather than linear increase.
5.4·Weakness
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Justification for using 11 g of coffee relies on a general literature value. Cite a primary source or perform a preliminary caffeine content assay for greater accuracy.
5.5·Strength
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Risk assessment thoroughly identifies hazards for DCM use, gloves and goggles are noted. This shows clear consideration of safety and environmental factors.
5.6·Weakness
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Disposal by slow evaporation in a fume hood may not comply with chemical waste regulations. Recommend following institutional solvent-waste protocols.
5.7·Strength
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Use of a drying agent is a strong methodological adaptation that reduced aqueous contamination and improved purity of the extract.
5.8·Weakness
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Bibliography entries show inconsistent styles and incomplete URLs. Apply a uniform citation format (e.g., APA, ACS) and verify all links.
Criteria A: Research Design
4/6
0
3
6
Criteria Strands
A.1Research question context
Excellent
A.2Methodological considerations
Good
A.3Methodology description
Good
Criteria Feedback
Research question stated within a specific and chemically appropriate context
Clear identification of independent, dependent, and controlled variables with basic justification
Methodology description allows reproducibility with few ambiguities
Rationale for choice of three replicates and total solvent volume is asserted rather than fully explained
Minor inconsistencies in sample mass description (55 g vs. 11 g) undermine clarity
The research question is clearly stated and framed within a specific context, linking caffeine polarity, partition behavior, and extraction cycles. This focus supports reproducibility and relevance.
1.2·Strength
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Background material concisely explains caffeine polarity and DCM characteristics, grounding the study in relevant chemical principles.
1.3·Suggestion
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The preliminary trials section documents methodological adjustments but omits justification for choosing three replicates. Explain why this sample size was considered sufficient.
1.4·Suggestion
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The table of DCM volumes per cycle is clear, but the rationale for a total 30 mL volume is not explained. Justify why this volume was chosen chemically.
1.5·Weakness
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Coffee solution preparation describes 55 g for 5 trials, but earlier sections reference 11 g per trial. Resolve this inconsistency to ensure reproducibility.
1.6·Suggestion
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Shaking 16 times is specified, but the basis for this number is unclear. Explain how this frequency was determined to balance mixing and emulsion control.
1.7·Weakness
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Carrying capacity L is set to the maximum observed mean but lacks theoretical justification. Discuss why saturation should occur at that value.
Criteria B: Data Analysis
4/6
0
3
6
Criteria Strands
B.1Communication of data recording and processing
Good
B.2Consideration of uncertainties
Moderate
B.3Data processing quality
Good
Criteria Feedback
Data tables and graphs are clearly presented with units, significant figures, and error bars
Processing methods (mean calculation, logarithmic linearisation, derivative analysis) are appropriate and yield a coherent trend
Uncertainties are propagated into means and transformed-data errors are reported
Decimal format is inconsistent (comma vs. point) and some table labels are missing or mislabeled
Instrument and sample uncertainties are not clearly separated in propagation formulas
Independent-variable uncertainty is ignored and logarithmic-model propagation is oversimplified
2.1·Weakness
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Weighing procedure uses three-digit scale uncertainty; random and systematic uncertainties should be separated in propagation for transparency.
2.2·Strength
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Calculated mass table is well organized with uncertainties and units clearly shown, facilitating precise interpretation.
2.3·Weakness
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Raw data table mixes comma and point separators and includes blank header cells. Use a consistent decimal format and tidy the columns.
2.4·Weakness
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Total uncertainty shows correct propagation formula but mislabels Uₜ twice. Distinguish instrument and sample uncertainties clearly.
2.5·Weakness
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Mean calculation uses range/2 for uncertainty but omits standard deviation. Include an analysis of spread (σ) to better assess precision.
2.6·Strength
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Table of uncertainties is comprehensive, presenting mean, absolute, and percentage uncertainties for each cycle clearly.
2.7·Weakness
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The percentage uncertainty formula uses commas in decimals (e.g., 7,7%). Adopt consistent use of decimal points to match SI conventions.
2.8·Suggestion
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Graph 2 would benefit from a residual plot or discussion of deviations from linearity to validate the model fit.
2.9·Suggestion
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Graph 1 lacks explicit axis labels and units, making it difficult to assess scale. Include full labeling for both axes.
2.10·Weakness
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Linearization table caption references ‘table blank.’ Ensure table numbering is correct and accompanying data is clearly labeled.
Criteria C: Conclusion
3/6
0
3
6
Criteria Strands
C.1Conclusion relevance and support
Good
C.2Scientific context comparison
Moderate
Criteria Feedback
Conclusion restates the research question and links findings to the logarithmic model and derivative-based optimum
Assertions are consistent with the processed results
Brief comparison to literature on coffee-ground extraction adds context
Over-interpretation of a continuous optimum (4.2 cycles) from discrete data is not discussed
Comparison to scientific literature is superficial and lacks quantitative reconciliation
Practical limitations of applying a continuous model to integer-cycle experiments are not addressed
3.1·Weakness
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Interpreting 4.2 cycles in practical terms overextends discrete cycle data. Discuss limitations of applying continuous models to integer‐cycle experiments.
3.2·Strength
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Conclusion restates findings clearly and links to analytical results. The use of logarithmic model and calculus adds depth to the interpretation.
Criteria D: Evaluation
3/6
0
3
6
Criteria Strands
D.1Methodological weaknesses
Moderate
D.2Suggested improvements
Moderate
Criteria Feedback
Identifies specific methodological weaknesses (trial number, volumetric accuracy, unknown caffeine content) and outlines their effects
Proposes realistic improvements such as increasing replicates, precise pipetting, standardized samples, and temperature control
Links suggested improvements to identified limitations
Does not quantify or rank the relative impact of each weakness on overall reliability
Lacks sensitivity analysis for the chosen 5 % optimisation threshold
Explanations of how each improvement addresses uncertainty are brief
4.1·Weakness
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The 5% optimization threshold is introduced without sensitivity analysis. Explain why this cutoff is chemically or economically justified.
4.2·Suggestion
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Weakness table effectively links specific limitations to results but does not rank their relative impact. Quantify which error sources most affect reliability.